| 摘要: |
| [目的]制定痛风止痛涂膜剂的质量标准,使其具有较好的质量可控性。[方法]以大黄对照药材为对照品,以苯-乙酸乙酯-甲酸-甲醇-水(30:10:0.5:2:5)的上层溶液为展开剂进行薄层色谱鉴别,并按有关规定进行常规检验。[结果]供试品(痛风止痛涂膜剂)色谱中,在与对照药材色谱相应的位置上,显相同颜色的斑点,阴性对照液无干扰;其他各检查项均符合相关规定。[结论]该方法简单易行、重现性好,可作为痛风止痛涂膜剂质量控制标准。 |
| 关键词: 痛风止痛涂膜剂 质量标准 薄层鉴别 |
| DOI：10.11656/j.issn.1673-9043.2005.03.08 |
| 分类号: |
| 基金项目: |
|
| Investigation on Quality Criteria of Arthrolithiasis Odynolysis Plastics |
|
CUI Wei-li
|
|
The First Affiliated Hospital to Tianjin University of TCM, Tianjin 300193, China
|
| Abstract: |
| [Objective] To instrtute the quality criteria on arthrolithiasis odynolysis plastics and make a better quality controllability.[Methods] The rhubarb was control article in the experiment.The developing agent was upper stratum solution of which comprised of benzeneacetidin-formic acid-methanol-water.To made an identify by thin layer chromatography (TLC) method and carry out routine analysis according to related regulation.[Results] The colour spectrum of arthrolithiasis odynolysis plastics showed up identical colour speckle in correspondling position with colour spectrum of control article.The negative control solution was non-interference and all the examination fitted with correlated regulation.[Conclusion] The method was simple,reasonable and owned a good reproducibility.The method may become the quality criteria of arthrolithiasis odynolysis plastics. |
| Key words: arthrolithiasis odynolysis plastics quality criteria lamella identify |
