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| Study on quality standard of Fushen granule |
| Hits 1957 Download times 1832 Received:April 17, 2011 |
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| DOI
10.11656/j.issn.1673-9043.2011.04.14 |
| Key Words
Fushen granule;TLC;HPLC;icariine;Radix Astragali;Radix Angelicae Sinensis;Radix Salviae Miltiorrhizae;Radix et Rhizoma Rhei;Pericarpium Citri Reticulatae |
| Author Name | Affiliation | | YAN Xue-mei | The First Hospital Affiliated to Tianjin University of TCM, Tianjin 300193, China | | JIA Fan | The First Hospital Affiliated to Tianjin University of TCM, Tianjin 300193, China |
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| Abstract
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| [Objective] To establish the quality standard of Fushen granule.[Methods] Radix Astragali,Radix Angelicae Sinensis,Radix Salviae Miltiorrhizae,Radix et Rhizoma Rhei and Pericarpium Citri Reticulatae in some preparations were identified qualitatively by TLC and the content of icariine in Herba Epimedii was determined by HPLC.[Results] The TLC spots were distinctive and specific.The linear range of quercetin,kaempferide, isorhamnetin was 0.048 5～0.97μg(r=0.999 9).The average recovery rate was 97.0%(RSD=0.7%).[Conclusion] The method is reliable,accurate,and reproducible for the quality control of Fushen granule. |
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