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| The research of quality contral of Jiawei Xianglian pill |
| Hits 2599 Download times 111 Received:July 11, 2016 |
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| DOI
10.11656/j.issn.1673-9043.2016.06.13 |
| Key Words
Jiawei Xianglian pill;TLC;HPLC;Paeoniflorin;Naringin;Baicalin;Magnolo |
| Author Name | Affiliation | E-mail | | ZHANG Xiao-xue | Tianjin university of Traditional Chinese Medicine, Tianjin 300193, China | | | WU Jie | Tianjin university of Traditional Chinese Medicine, Tianjin 300193, China | | | YU He-shui | Tianjin university of Traditional Chinese Medicine, Tianjin 300193, China | | | ZHANG Li-juan | Tianjin university of Traditional Chinese Medicine, Tianjin 300193, China | | | LI Wei | Tianjin university of Traditional Chinese Medicine, Tianjin 300193, China | | | SONG Xin-bo | Tianjin university of Traditional Chinese Medicine, Tianjin 300193, China
Tianjin Zhongyi pharmaceutical Co. Ltd, Tianjin 300193, China | songxinbo@tjutcm.edu.cn |
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| Abstract
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| [Objective] To research the quality control of Jiawei Xianglian pill.[Methods] Paeoniae Radix Alba,Angelicae Sinesis Radix and Scutellaria Radix of Jiawei Xianglian pill was identified by TLC.HPLC was applied to determine the content of paeoniflorin,naringin,baicalin and magnolol.[Results] TLC identification methods had good specificities without interference from negative control.The calibration curves of paeoniflorin,naringin,baicalin and magnolol were linear in the ranges of 0.011 68~0.116 8,0.022~0.22,0.255~0.025 5 and 0.004 1~0.041 mg/mL.The average recoveries wear 98.75%(RSD=1.63%),99.79%(RSD=1.3%),99.22%(RSD=1.57%),99.36%(RSD=1.6%).[Conclusion] This method was simple,pricise and repeatablewhich can be used for quality control of Jiawei Xianglian pill. |
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