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| Analysis of chemical constituents from Evodia rutaecarpa by UHPLC-Q-TOF-MS/MS |
| Hits 617 Download times 705 Received:August 20, 2022 |
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| DOI
10.11656/j.issn.1673-9043.2023.02.15 |
| Key Words
Evodia rutaecarpa;UHPLC-Q-TOF-MS/MS;component analysis |
| Author Name | Affiliation | E-mail | | LI Ming | Tangshan People's Hospital, Tangshan 063000, China | | | YUAN Jinbin | Jiangxi University of Traditional Chinese Medicine, Nanchang 330004, China | | | ZHANG Xun | Tangshan Union Hospital, Tangshan 063000, China | | | FENG Hao | Tangshan Union Hospital, Tangshan 063000, China | | | REN Xiaojing | Tangshan Union Hospital, Tangshan 063000, China | rxiaojing108054@126.com |
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| Abstract
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| [Objective] A rapid and sensitive UHPLC-Q-TOF-MS/MS method was used for qualitative analysis of chemical constituents of Evodia rutaecarpa.[Methods] The chromatographic conditions were ZORBAX Eclipse plus C18 column (2.1 mm×100 mm, 1.8 μm) with water (0.2% formic acid)-acetonitrile (0.2% formic acid) as mobile phase at the flow rate of 0.3 mL/min and column temperature of 30℃. Using electrospray ion source, positive and negative ion scanning detection, data in this study analysis by PeakView software.[Results] A total of 64 compounds were identified, including 42 alkaloids, 8 limonin, 8 flavone glycosides, 3 phenylpropanoids and 3 other compounds.[Conclusion] This experimental method can quickly and accurately analyze the chemical constituents of Evodia rutaecarpa, and lay a foundation for the study of the toxic components and pharmacodynamic components of Evodia rutaecarpa. |
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