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Research on Quality Control of Qingfei Yihuo Tablet |
Hits 1440 Download times 1548 Received:March 21, 2002 |
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DOI
10.11656/j.issn.1672-1519.2002.03.30 |
Key Words
HPLC;TLC;Huangqin glucoside;Dahuang;Zhizi |
Author Name | Affiliation | Li Jian | Tianjin Tasly Pharmaceutical Co. Ltd. Tianjin 300402, China | Xu Jinbo | Tianjin Tasly Pharmaceutical Co. Ltd. Tianjin 300402, China | Chen Yan | Tianjin Tasly Pharmaceutical Co. Ltd. Tianjin 300402, China | 林翠英 | 天津中医学院, 天津, 300193 |
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Abstract
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Objective: To study the quality control of Qingfei Yihuo Tablet. Methods: The main ingredients in this tablet were Huangqin glucoside, Dahuang and Zhizi. The content of Huangqin glucoside was examined with HPLC using ODS column, and methanol-water-phosphoric acid (50:60:0.2) as mobile phase. Dahuang and Zhizi were differentiated qualitatively with TLC. Results: The mean recovery rate was 101.2% and RSD 1.58% with HPLC. Clear atlas of qualitative differentiation and good reappearance were obtained with TLC. Conclusion: This method is convenient, practicable and has well specialty. So the quality can be controlled effectively. |
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