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| Content analysis of Anthraquinones in stir-baked semen cassiae by ultraviolet Spectrophotometry |
| Hits 2031 Download times 2226 Received:December 12, 2006 |
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| DOI
10.11656/j.issn.1672-1519.2007.02.32 |
| Key Words
semen cassiae;Cassia tora;anthraquinones;ultraviolet spectrophotometry |
| Author Name | Affiliation | | ZHOU Hong-yan | Nanjing University of TCM, Nanjing 210046, China | | CHEN Jian-wei | Nanjing University of TCM, Nanjing 210046, China |
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| Abstract
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| [Objective] To analyze anthraquinones contents in the stir-baked semen cassiae and find out a quantitative determination method for examining the effective content of anthraquinones in it. Simultaneously, the contents of anthraquinones in the crude and stir-baked ones from different districts are compared. [Methods] The ultraviolet spectrophotometry was used and the determination was performed at the wavelength of 513 nm. [Results] The linear relationship was fine(r=0.999 9) in 0.002 46～0.019 68 mg/ml. The recovery rate of anthraquinones was 96.973 8%, RSD=1.054 5%. [Conclusions] This method is simple and accurate. It can be used to detect the content of anthraquinones in the stir-baked semen cassiae. |
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