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| Determination of astragaloside Ⅳ in Qihuangjiangtang capsules with HPLC |
| Hits 1608 Download times 1784 Received:February 11, 2008 |
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| DOI
10.11656/j.issn.1672-1519.2008.05.28 |
| Key Words
Qihuangjiangtang capsules;Astragaloside Ⅳ;HPLC |
| Author Name | Affiliation | | HUANG Huai-peng | Hebei Ping’an Healthy Group Co. Ltd, Shijiazhuang 050021, China | | LIU Cai-xia | Hebei Ping’an Healthy Group Co. Ltd, Shijiazhuang 050021, China |
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| Abstract
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| [Objective] HPLC method was established to determine the contents of Astragaloside Ⅳ in Qihuangjiangtang capsules. [Methods] The samples were separated on a SinoChrom ODS-BP column (200 mm ×4.6 mm,5 μm) with the mobile phase of acetonitrile-water (36:64). The flow rate was 1.0 mL/min,and the detection wavelength was set at 203 nm. [Results] The linear ranges of Astragaloside Ⅳ was 20～400 mg/L (r=0.9997), the average recovery was 99.7%, RSD was 2.1%. [Conclusion] The method was accurate and sensitive with good reproducibility,so it can be an effective method to control the quality of Qihuangjiangtang capsules. |
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