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Studies of quality standard about Fufang Dangshen capsules |
Hits 1891 Download times 1470 Received:January 16, 2013 |
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DOI
10.11656/j.issn.1672-1519.2013.04.10 |
Key Words
Fufang Dangshen capsules;quality control;TLC;UV-spectrophotometry |
Author Name | Affiliation | 于春泉 | 天津中医药大学,天津 300193 | 王怡 | 天津中医药大学,天津 300193 | 陈薇 | 天津中医药大学第一附属医院,天津 300193 | 于立志 | 天津中医药大学,天津 300193 | 姜智浩 | 天津中医药大学,天津 300193 | 姬艳苏 | 天津中医药大学,天津 300193 |
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Abstract
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[Objective] To study and establish the quality control methods for Fufang Dangshen capsules.[Methods] The method of TLC was used to identify Radix Codonopsis,Rhizoma Atractylodis Macrocephalae,Rhizoma Cyperi and Sesami Semen Nigrun. The content of polysaccharose was determined by ultraviolet spectrophotometric method. [Results] Four herbal drugs were well identified by TLC,the spots were clear,round and without interference. Quantitative analysis of ultraviolet spectrophotometric method showed that the linear range of determination polysaccharose was 60.96~304.8 μg,r=0.999 5(n=8). The average recovery of determination was 99.79% and the RSD was 1.98% (n=6). [Conclusion] This method is simple,reliable and high specific with good repeatability,and can be used for the quality control of Fufang Dangshen capsules. |
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