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| Identification of the volatile components in different preparations of Xuefu Zhuyu by GC-MS |
| Hits 1844 Download times 1816 Received:October 13, 2015 |
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| DOI
10.11656/j.issn.1672-1519.2016.02.12 |
| Key Words
pace gas chromatography-mass spectrometry;Xuefu Zhuyu preparation;volatile component |
| Author Name | Affiliation | E-mail | | YU Hui-juan | Tianjin State Key Laboratory of Modern Chinese Medicine-Province and Ministry Co-established State Key Laboratory Cultivation Base, Institute of Traditional Chinese Medicine, Tianjin University of Traditional Chinese Medicine, Tianjin 300193, China
Research and Development Center of Traditional Chinese Medicine, Tianjin International Joint Academy of Biotechnology and Medicine, Tianjin 300457, China | | | YANG Fan | Tianjin State Key Laboratory of Modern Chinese Medicine-Province and Ministry Co-established State Key Laboratory Cultivation Base, Institute of Traditional Chinese Medicine, Tianjin University of Traditional Chinese Medicine, Tianjin 300193, China
Research and Development Center of Traditional Chinese Medicine, Tianjin International Joint Academy of Biotechnology and Medicine, Tianjin 300457, China | | | JIANG Zhen-zuo | Tianjin State Key Laboratory of Modern Chinese Medicine-Province and Ministry Co-established State Key Laboratory Cultivation Base, Institute of Traditional Chinese Medicine, Tianjin University of Traditional Chinese Medicine, Tianjin 300193, China
Research and Development Center of Traditional Chinese Medicine, Tianjin International Joint Academy of Biotechnology and Medicine, Tianjin 300457, China | | | WANG Yue-fei | Tianjin State Key Laboratory of Modern Chinese Medicine-Province and Ministry Co-established State Key Laboratory Cultivation Base, Institute of Traditional Chinese Medicine, Tianjin University of Traditional Chinese Medicine, Tianjin 300193, China
Research and Development Center of Traditional Chinese Medicine, Tianjin International Joint Academy of Biotechnology and Medicine, Tianjin 300457, China | wangyuefei_2006@hotmail.com | | YANG Xin-ying | Tianjin Hongrentang Pharmaceutical Co., Ltd., Tianjin 300385, China | |
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| Abstract
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| [Objective] To identify the volatile components in different preparations of Xuefu Zhuyu, a rapid GC-MS method was established.[Methods] Headspace gas chromatography-mass spectrometry(HS-GC/MS) was employed for identification of the components in Xuefu Zhuyu capsules, Xuefu Zhuyu soft capsules, Xuefu Zhuyu tablets and Xuefu Zhuyu oral liquid.The volatile components were retrieved by NIST-10 library, the relative percentage contents of which were calculated by area normalization method.[Results] The 21 volatile components were identified from Xuefu Zhuyu capsules, including acetic acid, benzaldehyde, ligustilide and 2-methyl-butanal etc.The 22 volatile components were identified in Xuefu Zhuyu tablets, including limonene, 3-methyl-butanal, ligustilide and 2-methyl-butanal etc.Ten and five volatile components were identified in Xuefu Zhuyu soft capsules and Xuefu Zhuyu oral liquid, respectively.[Conclusion] In this study, the method established can be used for the detection and analysis of volatile components in different preparation of Xuefu Zhuyu.The results could provide the basis for the quality control of preparation of Xuefu Zhuyu. |
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