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Analysis of short-chain fatty acids of fried medicated leaven by headspace gas chromatography mass spectrometry
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DOI   10.11656/j.issn.1672-1519.2017.02.18
Key Words   headspace gas chromatography mass spectrometry;fried medicated leaven;short-chain fatty acid
Author NameAffiliationE-mail
WU Dan Tianjin State Key Laboratory of Modern Chinese Medicine Province and Ministry Co-established State Key Laboratory Cultivation Base, Tianjin University of Traditional Chinese Medicine, Tianjin 300193, China
Research and Development Center of Traditional Chinese Medicine, Tianjin International Joint Academy of Biotechnology and Medicine, Tianjin 300457, China 
 
LIU Shuang Tianjin State Key Laboratory of Modern Chinese Medicine Province and Ministry Co-established State Key Laboratory Cultivation Base, Tianjin University of Traditional Chinese Medicine, Tianjin 300193, China
Research and Development Center of Traditional Chinese Medicine, Tianjin International Joint Academy of Biotechnology and Medicine, Tianjin 300457, China 
 
XIE Hong-zhen Chinese Traditional Medicine and Single Chinese Herb, Tianjin 300110, China  
DU Jie Tianjin State Key Laboratory of Modern Chinese Medicine Province and Ministry Co-established State Key Laboratory Cultivation Base, Tianjin University of Traditional Chinese Medicine, Tianjin 300193, China
Research and Development Center of Traditional Chinese Medicine, Tianjin International Joint Academy of Biotechnology and Medicine, Tianjin 300457, China 
 
YANG Jun-jun Tianjin State Key Laboratory of Modern Chinese Medicine Province and Ministry Co-established State Key Laboratory Cultivation Base, Tianjin University of Traditional Chinese Medicine, Tianjin 300193, China
Research and Development Center of Traditional Chinese Medicine, Tianjin International Joint Academy of Biotechnology and Medicine, Tianjin 300457, China 
 
WANG Yue-fei Tianjin State Key Laboratory of Modern Chinese Medicine Province and Ministry Co-established State Key Laboratory Cultivation Base, Tianjin University of Traditional Chinese Medicine, Tianjin 300193, China
Research and Development Center of Traditional Chinese Medicine, Tianjin International Joint Academy of Biotechnology and Medicine, Tianjin 300457, China 
wangyuefei_2006@hotmail.com 
Abstract
    [Objective] To establish a headspace gas chromatography mass spectrometry method for analysis of short-chain fatty acids (SCFAs) of fried medicated leaven. [Methods] Headspace gas chromatography mass spectrometry (HS-GC/MS) was applied for this study. Fried medicated leaven samples were sealed in the headspace bottle for analysis. [Results] By retrieving the National Institute of Standards and Technology (NIST) library, seven SCFAs was identified, including acetic acid, propionic acid, isobutyric acid, butyric acid, isovaleric acid, valeric acid and caproic acid. [Conclusion] The method could be used for rapid analysis of SCFAs of fried medicated leaven, which could establish the foundation for quality control of fried medicated leaven.

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