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| Study on volatile components in Zixue Powder by headspace gas chromatography mass spectrometry |
| Hits 399 Download times 521 Received:August 04, 2022 |
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| DOI
10.11656/j.issn.1672-1519.2022.11.19 |
| Key Words
Zixue Powder;volatile component;headspace injection;gas chromatography mass spectrometry |
| Author Name | Affiliation | E-mail | | SONG Lingling | Institute of Chinese Medicine, Tianjin University of Traditional Chinese Medicine, Tianjin 301617, China
State Key Laboratory of Component-based Chinese Medicine, Tianjin University of Traditional Medicine, Tianjin 301617, China
Tianjin Key Laboratory of Traditional Chinese Medicine Chemistry and Analysis, Tianjin 301617, China | | | MU Qixuan | Institute of Chinese Medicine, Tianjin University of Traditional Chinese Medicine, Tianjin 301617, China
State Key Laboratory of Component-based Chinese Medicine, Tianjin University of Traditional Medicine, Tianjin 301617, China
Tianjin Key Laboratory of Traditional Chinese Medicine Chemistry and Analysis, Tianjin 301617, China | | | WANG Fan | Tianjin Hongrentang Pharmaceutical Co., Ltd., Tianjin 300385, China | | | ZHANG Hui | Tianjin Hongrentang Pharmaceutical Co., Ltd., Tianjin 300385, China | | | CHAI Xin | Institute of Chinese Medicine, Tianjin University of Traditional Chinese Medicine, Tianjin 301617, China
State Key Laboratory of Component-based Chinese Medicine, Tianjin University of Traditional Medicine, Tianjin 301617, China
Tianjin Key Laboratory of Traditional Chinese Medicine Chemistry and Analysis, Tianjin 301617, China | | | WANG Yuefei | Institute of Chinese Medicine, Tianjin University of Traditional Chinese Medicine, Tianjin 301617, China
State Key Laboratory of Component-based Chinese Medicine, Tianjin University of Traditional Medicine, Tianjin 301617, China
Tianjin Key Laboratory of Traditional Chinese Medicine Chemistry and Analysis, Tianjin 301617, China | | | CUI Ying | Institute of Chinese Medicine, Tianjin University of Traditional Chinese Medicine, Tianjin 301617, China
State Key Laboratory of Component-based Chinese Medicine, Tianjin University of Traditional Medicine, Tianjin 301617, China
Tianjin Key Laboratory of Traditional Chinese Medicine Chemistry and Analysis, Tianjin 301617, China | CQL8179270@tjutcm.edu.cn |
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| Abstract
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| [Objective] To establish a rapid analytical method for identifying the volatile components in Zixue Powder by headspace gas chromatography mass spectrometry(HS GC-MS) and evaluate the difference of the volatile components among different batches and different processes of Zixue Powder sample.[Methods] The analytical method of volatile components in Zixue Powder was established by HS GC-MS. The compounds were identified by NIST 17 database retrieval and traced to the herbal sources. The relative content of each compound was determined by peak area normalization method.[Results] The 46 volatile compounds were characterized from Zixue Powder,including alcohols,esters,aldehydes,ketones,acids,hydrocarbons and nitrogenous compounds,and the main compound was muscone. There were great differences in the relative content of the volatile components among different batches and processes of Zixue Powder sample.[Conclusion] The volatile components in Zixue Powder were characterized,which provides a basis for scientific evaluation and effective quality control of Zixue Powder. |
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