| 摘要: |
| [目的] 研究制备芒果苷磷脂复合物的最佳制备工艺。[方法] 以芒果苷与磷脂的复合率为评价标准,采用单因素考察和正交实验筛选工艺参数。[结果] 确定了制备芒果苷磷脂复合物的最佳工艺条件:以甲醇-丙酮为反应溶剂,芒果苷质量浓度为0.25 g/L,物料比摩尔比为1:1,反应温度为40 ℃,反应时间为2 h.[结论] 优化工艺可制得复合率较高的芒果苷磷脂复合物,简单可行。 |
| 关键词: 芒果苷 磷脂复合物 制备工艺 |
| DOI：10.11656/j.issn.1672-1519.2012.01.27 |
| 分类号: |
| 基金项目:天津市高等学校科技发展基金计划项目(20100211). |
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| Study on preparation method of mangiferin phospholipid complex |
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TIAN Hui, WANG Ya-jing, SUN Shi-zhen, WANG Yan-ming, PENG Shu-juan, GAO Xu
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Tianjin University of TCM, Tianjin State Key Laboratory of Modern Chinese Medicine, Tianjin 300193, China
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| Abstract: |
| [Objective] To determine the best technology for preparing Mangiferin phospholipids complex. [Methods] The compounding rate of mangiferin and phospholipid was investigated with mono-agent investigation and orthogonal design test to analyze the technological parameters. [Results] The best conditions for preparing mangiferin phospholipid complex were as follows: methanol and acetone were used as reaction solvent, concentration of mangiferin in solvent was 0.25 g/L, molar ratio of mangiferin and phospholipid was 1:1, react was performed for 2.0 hr at 40 ℃。 [Conclusion] The optimized preparing technology can get mangiferin phospholipid complex with a high compounding rate. The technology is easy and feasible. |
| Key words: mangiferin phospholipid complex preparation method |
