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| 血府逐瘀颗粒薄层色谱鉴别方法的研究 |
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刘征辉1,2, 叶挺祥1,2, 赵琳琳1,2, 郭永泽1,2, 程奕1,2, 罗国安3
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1.天津海世达检测技术有限公司, 天津 300381;2.天津市现代中药质量检验中心, 天津 300381;3.清华大学化学系, 北京 100084
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| 摘要: |
| [目的] 研究改进血府逐瘀颗粒的薄层色谱鉴别方法。[方法] 采用薄层色谱法对成药中的当归、川芎、甘草、牛膝、枳壳进行定性鉴别。[结果] 薄层色谱鉴别的色谱斑点清晰,阴性空白无干扰。[结论] 所建立的鉴别方法专属性强,方法可靠,可作为血府逐瘀颗粒的定性控制方法。 |
| 关键词: 当归 川芎 甘草 牛膝 枳壳 薄层色谱法 |
| DOI：10.11656/j.issn.1672-1519.2012.03.29 |
| 分类号: |
| 基金项目:天津市科技发展计划项目(05SYSYGX25000). |
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| Identification of Xuefu Zhuyu granule with TLC method |
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LIU Zheng-hui1,2, YE Ting-xiang1,2, ZHAO Lin-lin1,2, GUO Yong-ze1,2, CHENG Yi1,2, LUO Guo-an3
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1.Tianjin Highshida Quality Testing Limited Company, Tianjin 300381, China;2.Tianjin Center for Quality Testing of TCM, Tianjin 300381, China;3.Department of Chemistry, Qinghua University, Beijing 100084, China
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| Abstract: |
| [Objective] To improve the differentiating method of Xuefu Zhuyu granule with TLC. [Methods] Radix Angelica Sinensis, Rhizoma Chuanxiong, Radix Glycyrrhiza, Radix Achyranthis Bidentatae, Fructus aurantii in Xuefu Zhuyu granule were identified by TLC. [Results] The developed TLC spots were quite clear and the negative blank solution had no interference. [Conclusion] The method of identification is specific, reliable, and can be a quality-controlling method for this granule. |
| Key words: Radix Angelica Sinensis Rhizoma Chuanxiong Radix Glycyrrhiza Radix Achyranthis Bidentatae Fructus aurantii TLC |
